Pendugaan umur simpan sediaan bawang tunggal hitam dengan metode accelerated shelf-life testing (ASLT)

Gunawan Priadi; Fitri Setiyoningrum; Fifi Afiati; Hisaqia Amieni; Muhamad Arpah

doi:10.24960/jli.v9i2.5454.79-88

Pendugaan umur simpan sediaan bawang tunggal hitam dengan metode accelerated shelf-life testing (ASLT)

Gunawan Priadi, Fitri Setiyoningrum, Fifi Afiati, Hisaqia Amieni, Muhamad Arpah

Abstract

Sediaan bawang tunggal hitam terdiri atas bawang tunggal hitam utuh, ekstrak dan mikroenkapsulat. Senyawa antioksidan dalam sediaan bawang tunggal hitam akan mengalami kerusakan selama penyimpanan. Penelitian ini bertujuan menentukan kinetika degradasi kapasitas antioksidan dan total fenolik pada sediaan bawang tunggal hitam dan memperkirakan umum simpannya dengan metode accelerated shelf-life testing (ASLT). Hasil penelitian menunjukan kapasitas antioksidan dan total fenolik sediaan bawang tunggal hitam mengalami penurunan selama penyimpanan. Total fenolik dijadikan parameter penentuan umur simpan sediaan bawang tunggal hitam. Bawang tunggal hitam utuh mengalami kerusakan lebih cepat dibandingkan sediaan lainnya. Umur simpan sediaan bawang tunggal hitam pada suhu 25°C adalah: bawang tunggal hitam utuh 199 hari, ekstrak bawang tunggal hitam 259 hari, dan mikroenkapsulat 255 hari.

ABSTRACT

Solo black garlic products consisted of whole solo black garlic, extract, and microencapsulated. Antioxidant compounds in the black garlic products will be damaged during storage. The study was aimed to determine the kinetics degradation of antioxidant capacity and total phenolic of black garlic products and to estimate their shelf life using accelerated shelf life testing (ASLT) method. The result showed that antioxidants and total phenolic of products decreased during storage. Total phenolic was used to predict the shelf life of products. The whole black garlic deterioration is faster than other products. The shelf life of whole black garlic, black garlic extract and microencapsulated black garlic extract at 25°C were 199 days, 259 days, and 255 days respectively.

Keywords

antioksidan; Arrhenius; senyawa fenolik; konstanta reaksi

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References

Afanas’ev, I.B., Dcrozhko, A.I., Brodskii, A. V., Kostyuk, V.A., Potapovitch, A.I., 1989. Chelating and free radical scavenging mechanisms of inhibitory action of rutin and quercetin in lipid peroxidation. Biochem. Pharmacol. 38, 1763–1769. https://doi.org/10.1016/0006-2952(89)90410-3

Agoes, G., 2007. Teknologi bahan alam. ITB Press, Bandung.

Arif, A. Bin, 2016. Metode accelarated shelf life test (ASLT) dengan pendekatan arrhenius dalam pendugaan umur simpan sari buah nanas pepaya dan cempedak. Inform. Pertanian, 25, 189–198. https://doi.org/10.3989/sefarad.011.001

Arpah, M., 2007. Penetapan kadaluwarsa pangan. Departemen Ilmu dan Teknologi Pangan Institut Pertanian Bogor, Bogor.

Asiah, N., Cempaka, L., David, W., 2018. Panduan praktis pendugaan umur simpan Produk pangan. Universitas Bakrie, Jakarta.

Bae, S.E., Cho, S.Y., Won, Y.D., Lee, S.H., Park, H.J., 2014. Changes in S-allyl cysteine contents and physicochemical properties of black garlic during heat treatment. LWT - Food Sci. Technol. 55, 397–402. https://doi.org/10.1016/j.lwt.2013.05.006

Bae, S.E., Cho, S.Y., Won, Y.D., Lee, S.H., Park, H.J., 2012. A comparative study of the different analytical methods for analysis of S-allyl cysteine in black garlic by HPLC. LWT - Food Sci. Technol. 46, 532–535. https://doi.org/10.1016/j.lwt.2011.11.013

Budijanto, S., Sitanggang, A.B., Silalahi, B.E., Murdiati, W., 2010. Penentuan umur simpan seasoning menggunakan metode accelerated shelf-life testing (ASLT) dengan pendekatan kadar air kritis. J. Teknol. Pertan. 11, 71–77.

Capuano, E., Fogliano, V., 2011. Acrylamide and 5-hydroxymethylfurfural (HMF): A review on metabolism, toxicity, occurrence in food and mitigation strategies. LWT - Food Sci. Technol. 44, 793–810. https://doi.org/10.1016/j.lwt.2010.11.002

Choi, I.S., Cha, H.S., Lee, Y.S., 2014. Physicochemical and antioxidant properties of black garlic. Molecules 19, 16811–16823. https://doi.org/10.3390/molecules 191016811

Chu, Q., Lee, D.T.W., Tsao, S.W., Wang, X., Wong, Y.C., 2007. S-allylcysteine, a water-soluble garlic derivative, suppresses the growth of a human androgen-independent prostate cancer xenograft, CWR22R, under in vivo conditions. BJU Int. 99, 925–932. https://doi.org/10.1111/j.1464-410X.2006. 06639.x

Diniyah, N., Subagio, A., Akhiriani, A., 2015. Pendugaan umur simpan “beras cerdas” berbasis mocaf, tepung jagung menggunakan metode accelerated shelf-life testing (ASLT) pendekatan Arrhenius. J. Agro-based Ind. 32, 1–8.

Gitalasa, F., Rostini, I., Pratama, R.I., 2018. Estimation of shelf life using accelerated shelf life test (ASLT) method Arrhenius model on sheet nile Tilapia Jerky. Glob. Sci. J. 6, 62–69.

Ha, A.W., Ying, T., Kim, W.K., 2015. The effects of black garlic (Allium satvium) extracts on lipid metabolism in rats fed a high fat diet. Nutr. Res. Pract. 9, 30–36. https://doi.org/10.4162/nrp.2015.9. 1.30

Handayani, S.N.U.R., Bawono, L.C., Pramesti, D., Pratiwi, H.N., 2018. Isolasi senyawa polifenol black garlic dan uji toksisitasnya terhadap larva udang (Artemia salina Leach). J. Ilmu Kefarmasian Indones. 16, 145–149.

Haouet, M.N., Tommasino, M., Mercuri, M.L., Benedetti, F., Di Bella, S., Framboas, M., Pelli, S., Altissimi, M.S., 2018. Experimental accelerated shelf life determination of a ready-to-eat processed food. Ital. J. Food Saf. 7, 189–192. https://doi.org/10.4081/ijfs.2018.6919

Hariyadi, P., 2004. Prinsip-prinsip pendugaan masa kadaluwarsa dengan metode accelerated shelf life test. Pusat Studi Pangan dan Gizi Bogor Institut Pertanian Bogor, Bogor.

Herawati, H., 2008. Penentuan umur simpan pada produk pangan. Litbang Pertan. 27, 124–130.

Iriani, E.S., Widayanti, S.M., Miskiyah, M., Juniawati, J., 2014. Pengaruh ekstrak bawang putih terenkapsulasi terhadap karakteristik kemasan antimikroba. J. Kim. dan Kemasan 36, 271. https://doi.org/10.24817/jkk.v36i2.1895

Javanmardi, J., Stushnoff, C., Locke, E., Vivanco, J.M., 2003. Antioxidant activity and total phenolic content of Iranian Ocimum accessions. Food Chem. 83, 547–550. https://doi.org/10.1016/S0308-8146(03)00151-1

Jedermann, R., Nicometo, M., Uysal, I., Lang, W., 2014. Reducing food losses by intelligent food logistics. Philos. Trans. R. Soc. A Math. Phys. Eng. Sci. 372. https://doi.org/10.1098/rsta.2013.0302

Jeong, Y.Y., Ryu, J.H., Shin, J.H., Kang, M.J., Kang, J.R., Han, J., Kang, D., 2016. Comparison of anti-oxidant and anti-inflammatory effects between fresh and aged black garlic extracts. Molecules 21, 1–15. https://doi.org/10.3390/molecules21040430

Kähkönen, M.P., Hopia, A.I., Vuorela, H.J., Rauha, J.P., Pihlaja, K., Kujala, T.S., Heinonen, M., 1999. Antioxidant activity of plant extracts containing phenolic compounds. J. Agric. Food Chem. 47, 3954–3962. https://doi.org/10.1021/jf990146l

Kappel, V.D., Costa, G.M., Scola, G., Silva, F.A., Landell, M.F., Valente, P., Souza, D.G., Vanz, D.C., Reginatto, F.H., Moreira, J.C.F., 2008. Phenolic content and antioxidant and antimicrobial properties of fruits of Capsicum baccatum L. var. pendulum at different maturity stages. J. Med. Food 11, 267–274. https://doi.org/10.1089/jmf.2007.626

Kim, I., Kim, Jin-young, Hwang, Y., Hwang, K., Om, A., Kim, Jae-hyun, Cho, K., 2011. The beneficial effects of aged black garlic extract on obesity and hyperlipidemia in rats fed a high-fat diet. J. Med. Plants Res. 5, 3159–3168.

Kim, J.S., Kang, O.J., Gweon, O.C., 2013. Comparison of phenolic acids and flavonoids in black garlic at different thermal processing steps. J. Funct. Foods 5, 80–86. https://doi.org/10.1016/j.jff.2012.08.006

Kimura, S., Tung, Y.C., Pan, M.H., Su, N.W., Lai, Y.J., Cheng, K.C., 2017. Black garlic: A critical review of its production, bioactivity, and application. J. Food Drug Anal. 25, 62–70. https://doi.org/10.1016/j.jfda. 2016.11.003

Kurniadi, M., Bintang, R., Kusumaningrum, A., Nursiwi, A., Nurhikmat, A., Susanto, A., Angwar, M., Triwiyono, Frediansyah, A., 2017. Shelf life prediction of canned fried-rice using accelerated shelf life testing (ASLT) arrhenius method, in: IOP Conference Series: Earth and Environmental Science. p. 012029. https://doi.org/10.1088/1755-1315/

Lee, Y.-M., Gweon, O.-C., Seo, Y.-J., Im, J., Kang, M.-J., Kim, M.-J., Kim, J.-I., 2009. Antioxidant effect of garlic and aged black garlic in animal model of type 2 diabetes mellitus. Nutr. Res. Pract. 3, 156. https://doi.org/10.4162/nrp.2009.3.2.156

Liu, Q., Tang, G.-Y., Zhao, C.-N., Gan, R.-Y., Li, H.-B., 2019. Antioxidant activities,phenolic profiles, and organic acid contents of fruit vinegars. Antioxidants 8, 78. https://doi.org/10.3390/antiox8040078

Lu, X., Li, N., Qiao, X., Qiu, Z., Liu, P., 2017. Composition analysis and antioxidant properties of black garlic extract. J. Food Drug Anal. 25, 340–349. https://doi.org/10.1016/j.jfda.2016.05.011

Muanda, F., Kone, D., Dicko, A., Soulimani, R., Younos, C., 2011. Phytochemical composition and antioxidant capacity of three malian medicinal plant parts. Evidence-Based Complement. Altern. Med. 2011, 1–7. https://doi.org/10.1093/ecam/nep109

Muliadi, 2019. Pendugaan umur simpan buah alpukat (Persea americanamill) berdasarkan total padatan terlarut menggunakan model arrhenius dan Q10. Universitas Syah Kuala.

Mulyono, A., Afriyanti, Basuki, J., Sukaryani, S., 2018. Pendugaan umur simpan sirum buah tin “ Kharomah” dengan metode accelerated shelf life testing (ASLT). J. Ilmu dan Teknol. Pangan 4, 277–282.

Ngan, N., Giang, M., Tu, N., 2017. Biological activities of black garlic fermented with lactobacillus plantarum PN05 and some kinds of black garlic presenting inside vietnam. Indian J. Pharm. Educ. Res. 51, 672–678. https://doi.org/10.5530/ijper. 51.4.99

Park, C., Park, S., Chung, Y.H., Kim, G.Y., Choi, Y.W., Kim, B.W., Choi, Y.H., 2014. Induction of apoptosis by a hexane extract of aged black garlic in the human leukemic U937 cells. Nutr. Res. Pract. 8, 132–137. https://doi.org/10.4162/nrp.2014.8.2.132

Parsetiorini, O.E., 2011. Pendugaan umur simpan seasoning dan microencapsulated ginger powder dengan metode accelerated shelf life testing di PT Indesso Aroma. Institut Pertanian Bogor.

Patras, A., Brunton, N., Da Pieve, S., Butler, F., Downey, G., 2009. Effect of thermal and high pressure processing on antioxidant activity and instrumental colour of tomato and carrot purées. Innov. Food Sci. Emerg. Technol. 10, 16–22. https://doi.org/10.1016/j.ifset.2008.09.008

Pranoto, Y., Marseno, D.W., Teknologi, J., Pertanian, H., Pertanian, F.T., Mada, U.G., No, J.F., 2012. Perkiraan umur simpan kacang rendah lemak dilapisi dengan carboximethyl celulose menggunakan metode accelerated shelf-life test (ASLT). Agritech 32, 301–307.

Puri, R.Y.A., Wijana, S., Pranowo, D., 2018. Analisis kualitas sirup baby java pada stasiun proses dan pendugan umur simpan skala pilot plan. J. Teknol. Pertan. 19, 125–138.

Purnamayati, L., Dewi, E.N., Kurniasih, R.A., 2016. Karakteristik fisik mikrokapsul fikosianin spirulina pada konsentrasi bahan penyalut yang berbeda. J. Teknol. Has. Pertan. 9, 1–8. https://doi.org/ 10.20961/jthp.v9i2.12844

Rahmawati, F., 2017. Pendugaan umur simpan mikroenkapsulat ekstrak dan tepung kulit buah manggis dengan metode accelerated shelf-life testing (aslt) faradis rahmawati. Institut Pertanian Bogor.

Rahmi, S., Ahmad, U., Wulandari, D., 2016. Pendugaan umur simpan benih kedelai menggunakan metode accelerated shelf-life testing (ASLT). J. Keteknikan Pertan. 4, 75–80. https://doi.org/10.19028/jtep.04. 1.75-80

Rehman, R., Akram, M., Akhtar, N., Jabeen, Q., Shah, S.M.A., 2011. Zingiber officinale Roscoe (pharmacological activity). J. Med. Plants Res. 5, 344–348.

Reis, A.S. dos, Diedrich, C., Moura, C. de, Pereira, D., Almeida, J. de F., Silva, L.D. da, Plata-Oviedo, M.S.V., Tavares, R.A.W., Carpes, S.T., 2017. Physico-chemical characteristics of microencapsulated propolis co-product extract and its effect on storage stability of burger meat during storage at −15 °C. LWT - Food Sci. Technol. 76, 306–313. https://doi.org/10.1016/j.lwt.2016.05.033

Setyadjit, Sukasih, E., Arif, A. Bin, 2017. Prediction of storage life of shallot powder by using acceleration method. Int. J. Agric. Syst. 5, 140–153. https://doi.org/10.20956/ijas.v5i2.1236

Solco, A.K.S., 2007. Accelerated shelf-life test of alkamides in Echinacea purpurea root aqueous ethanol Soxhlet extracts. Iowa state University.

Steele, R. (Ed.), 2000. Temperature and food stability: analysis and control, in: Understanding and measuring the shelf-life of food. CRC Press LLC, pp. 42–65.

Susanti, M., 2008. Mikroenkapsulasi oleoresin daun sirih (Piper betle L.) untuk produksi bandeng (Chanos-chanos forsk) tinggi lisin pada proses pengasapan cair. J. Litbang Provinsi Jawa Teng. 6, 38–51.

Vermerris, W., Nicholson, R., 2008. Phenolic compound biochemistry, 1st ed. Springer Science + Business Media B.V, USA.

Wang, W., Sun, Y., 2017. In vitro and in vivo antioxidant activities of polyphenol extracted from black garlic. Food Sci. Technol. 37, 681–685. https://doi.org/10.1590/1678-457x.30816

Wungkana, I., Suryanto, E., Momuat, L., 2013. Aktivitas antioksidan dan tabir surya fraksi fenolik dari limbah tongkol jagung (Zea mays L.). Pharmacon 2, 149–155.

Zhang, X., Li, N., Lu, X., Liu, P., Qiao, X., 2016. Effects of temperature on the quality of black garlic. J. Sci. Food Agric. 96, 2366–2372. https://doi.org/ 10.1002/jsfa.7351

DOI: http://dx.doi.org/10.24960/jli.v9i2.5454.79-88